By Robert B. Bates,William A. Beavers

ISBN-10: 0896030105

ISBN-13: 9780896030107

ISBN-10: 0896030164

ISBN-13: 9780896030169

With the arrival of Fourier remodel spectrometers of serious sensitivity, it has develop into sensible to acquire carbon-13 nuclear magnetic resonance (C-13 NMR; l3C NMR; CMR) spectra normally on natural molecules, and this system has develop into one of many maximum software in picking buildings of natural unknowns. while the standard spectrometric recommendations­ proton magnetic resonance (H-I NMR; IH NMR; PMR), infrared (lR), mass (MS), and ultraviolet (UV)-do no longer comfortably show a compound's constitution, a C-13 NMR spectrum will frequently supply adequate additional info to yield it unequivocally. With this in brain, the current paintings used to be designed to provide complex undergraduates, graduate scholars, and practising chemists a operating wisdom of and facility with using this priceless procedure. a few familiarity with different spectrometric options is thought (recommended publication: Silverstein, Bassler, and Morrill, Spectrometric id of natural Compounds), yet no previous wisdom of C-13 NMR -which is taken care of very frivolously, if in any respect, within the accepted trouble-free natural texts-is helpful. A dialogue of C-13 NMR spectroscopy is via one hundred twenty five difficulties, every one along with a molecular formulation, kinds of C-13 NMR spectra (partially and entirely proton decoupled, with connecting traces to facilitate multiplicity assignments), an built-in H-I NMR spectrum, and crucial IR, UV, and MS facts. those difficulties were very rigorously ready, completely validated via scholars on the collage of Arizona, and we think that only a few mistakes remain.

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Carbon-13 NMR Spectral Problems (Organic Chemistry) by Robert B. Bates,William A. Beavers

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